专题论文

粉煤灰提纯莫来石制备的陶瓷材料组织及性能

  • 范磊 ,
  • 谭飞虎 ,
  • 陈平 ,
  • 陈华辉 ,
  • 曹洪治
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  • 1. 中国矿业大学(北京)机电与信息工程学院, 北京100083;
    2. 北京科技大学机械工程学院, 北京100083
范磊,工程师,研究方向为摩擦磨损理论及先进耐磨材料,电子信箱:fanlei@cumtb.edu.cn

收稿日期: 2013-09-02

  修回日期: 2013-12-11

  网络出版日期: 2014-04-10

基金资助

国家自然科学基金项目(51305023)

Microstructrue and Properties of Mullite-ceramics Synthesized from Fly Ash

  • FAN Lei ,
  • TAN Feihu ,
  • CHEN Ping ,
  • CHEN Huahui ,
  • CAO Hongzhi
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  • 1. School of Mechanical Electronic & Information Engineering, China University of Mining & Technology, Beijing 100083, China;
    2. School of Mechanical Engineering, University of Science and Technology Beijing, Beijing 100083, China

Received date: 2013-09-02

  Revised date: 2013-12-11

  Online published: 2014-04-10

摘要

利用粉煤灰提纯莫来石制备陶瓷材料,不仅可以降低生产成本,也可以减少粉煤灰堆积带来的环境危害。以不同化学成分的粉煤灰提纯莫来石粉为原料,通过球磨、压制、烧结制得陶瓷材料。探讨了烧结温度、成分对莫来石微晶陶瓷材料的体收缩率、烧失率、表观密度、冲击韧性、显微硬度的影响,分析了所制备陶瓷材料的显微结构特点。研究表明,在1450℃下进行烧结,制得的莫来石陶瓷材料最致密,体收缩率、显微硬度最大;S 型样品制得的试样致密度更高,综合性能较好;S 型中氧化钙含量多,降低了莫来石陶瓷材料的冲击韧性。

本文引用格式

范磊 , 谭飞虎 , 陈平 , 陈华辉 , 曹洪治 . 粉煤灰提纯莫来石制备的陶瓷材料组织及性能[J]. 科技导报, 2014 , 32(9) : 36 -40 . DOI: 10.3981/j.issn.1000-7857.2014.09.005

Abstract

To obtain the ceramics of mullite purified from fly ash not only cuts its production cost, but also improves the environment contaminated by the accumulation of fly ash. Through ball milling, pressing, sintering, the ceramic materials are prepared with different chemical compositions of mullite powders purified from the fly ash. This paper studies the influences of the sintering temperature and the composition of the microcrystalline mullite ceramics on the body shrinkage, the ignition loss, the apparent density, the impact toughness, the Vickers microhardness and the microstructure of the prepared ceramics. It is shown that with sintering mullite at 1450℃the obtained ceramic material has the most dense body shrinkage, the maximum Vickers microhardness; the sample prepared from the S type samples has an even greater density and the optimum overall performance; but the S-type sample has a large calcium oxide content and is not conducive to the impact toughness of the mullite ceramic materials.

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